EVAPORATION TO THE SPECIFIC GRAVITY DESIRED

Manufacturers of tomato pulp have considerable difficulty in securing

a product of uniform concentration and in determining at what point

to stop evaporation. Some manufacturers turn off the steam when it is

believed that the concentration has gone far enough and make a hasty

determination of specific gravity. If it is found the concentration

is not as great as is desired, heating is resumed for a time and the

specific gravity again determined. Others make but one determination

of specific gravity when it is believed that the desired concentration

has been reached, and if it is found to be underconcentrated, continue

the evaporation for a length of time which experience has indicated to

be necessary. Neither of these methods of operating is satisfactory.

They involve a great deal of work and the concentration of the product

obtained is not sufficiently uniform. Moreover, the determination of

specific gravity of hot pulp is very inaccurate (see p. 44).

A method of employing a gauge stick is believed to be simpler and more

practicable.

Some manufacturers who desire to work with the simplest possible

methods, even at the sacrifice of a high degree of control over the

concentration of their products, measure the volume of cyclone juice

introduced into the evaporating tank; and when it is believed that

the concentration is sufficient, measure the depth of the evaporated

product in the tank, the steam being momentarily turned off for that

purpose and the measurement being taken after the foam subsides. This

method was outlined in detail in a trade paper article published from

this laboratory in 1918. The method is somewhat inaccurate, because

it is based on the measurement of cyclone juice as it flows from the

cyclone and which therefore contains a large amount of air. This air

materially increases the volume of the pulp and consequently the

amount of finished pulp calculated from the volume of cyclone juice

containing this air is greater than can actually be obtained. Some

manufacturers of pulp have found the method practicable, however, by

making a correction based on factory experience on the amount of pulp

which the method indicates should result from the evaporation of each

bath. This method also calls for the use of measuring tanks, which

many manufacturers do not have and do not care to provide. The method

is therefore not repeated here, but the laboratory has a number of

reprints of the trade paper article which are available to any who

desire more detailed information regarding the matter.

The following method has been found more accurate and more convenient

than the one mentioned above. It has the special advantage that it is

based on the examination of the cyclone juice after the juice has been

heated to a sufficient extent to “break” the foam.

In using this method, the manner in which the cyclone juice is prepared

is immaterial. The tomatoes may be broken by steam or mechanical

breaker and may be cycloned hot or cold. The steam may be turned into

the coils as soon as they are covered and the cyclone juice may run

into the evaporating tank until the tank is filled.

Finally, when the last of the cyclone juice is added and the contents

of the tank are boiling vigorously, the steam is momentarily turned

off. The volume is then determined by means of a gauge stick and a

sample is withdrawn, filtered and the specific gravity or degrees Brix

determined as described on page 50. The extent to which evaporation

must be continued to secure pulp of the desired specific gravity is

determined by Table 9.

This table gives in the first four columns the specific gravity of the

partially concentrated pulp taken from the evaporating tank, the per

cent of solids of the same, the specific gravity of the filtrate and

the Brix reading of the filtrate. In order to use the tables, it is

only necessary to make use of one of these columns.

This method of operation can be simplified and more accurate results

obtained by equipping each evaporating tank with a one-inch gage glass

extending the full height of the tank. The gage glass should be open at

the top and connected with the bottom of the tank by a pipe equipped

with a valve. Before the tank is filled with cyclone juice the valve is

turned off and the gage glass filled with water. Steam is turned on as

soon as the pipes are covered and the foam is “broken” quickly without

trouble that was experienced in heating the tank filled with cool pulp.

The heat is continued while the tank is filled to the desired height

with the pulp. The steam is then momentarily turned off and the valve

at the top of the gage glass opened to permit the water in the gage

glass to equalize in height with the partly concentrated pulp within

the tank. The height of water in the gage glass is read by a scale

attached, the sample of the pulp taken for examination and the steam

again turned on.

There is ample time to determine the specific gravity of the sample of

partly concentrated pulp and from its volume as obtained by the gage

glass to calculate the volume to which the pulp should be evaporated

to secure the desired specific gravity in the finished product. The

specific gravity of the sample may be taken by any of the methods

described in the chapter on “Determination of specific gravity.” More

accurate results can be obtained by pouring the sample of pulp as soon

as it is taken into a large loosely stoppered flask and holding the

flask with constant agitation in a tub of ice water until it is brought

to about the temperature of the room.

Having determined the volume (when heated to the boiling point) of a

batch of cyclone juice or of pulp at any stage of its manufacture and

its specific gravity (at 68° F.), each of the last five columns of the

table gives a factor by which the volume of the partially evaporated

pulp may be multiplied to determine the volume of pulp of the specific

gravity given at the top of the column. Since both measurements are

taken at the boiling point the question of temperature need not be

considered.

Table 8.—_Corrections for Specific Gravity and Brix_[19] _Readings at

Different Temperatures to 68 Degrees F._ (_20 Degrees C._)

Corrections to be subtracted from specific gravity or degrees Brix.

===============+=============

Temperature | Corrections

-------+-------+-------+-----

Deg. F.|Deg. C.|Sp. Gr.|Brix.

-------+-------+-------+-----

50 | 10.0 | .0017 | .38

51 | 10.6 | .0016 | .36

52 | 11.1 | .0016 | .35

53 | 11.7 | .0015 | .33

54 | 12.2 | .0014 | .31

| | |

55 | 12.8 | .0014 | .30

56 | 13.3 | .0013 | .28

57 | 13.9 | .0012 | .26

58 | 14.4 | .0011 | .24

| | |

59 | 15.0 | .0010 | .22

60 | 15.6 | .0009 | .20

61 | 16.1 | .0009 | .18

62 | 16.7 | .0008 | .16

63 | 17.2 | .0007 | .13

| | |

64 | 17.8 | .0006 | .11

65 | 18.3 | .0004 | .08

66 | 18.9 | .0003 | .05

67 | 19.4 | .0002 | .03

69 | 20.6 | .0002 | .03

70 | 21.1 | .0003 | .05

71 | 21.7 | .0004 | .08

72 | 22.2 | .0006 | .11

73 | 22.8 | .0007 | .15

| | |

74 | 23.3 | .0009 | .18

75 | 23.9 | .0011 | .21

76 | 24.4 | .0012 | .24

77 | 25.0 | .0013 | .28

78 | 25.6 | .0015 | .32

| | |

79 | 26.1 | .0017 | .35

80 | 26.7 | .0018 | .39

81 | 27.2 | .0019 | .42

82 | 27.8 | .0021 | .46

83 | 28.3 | .0023 | .49

| | |

84 | 28.9 | .0024 | .54

85 | 29.4 | .0026 | .58

86 | 30.0 | .0027 | .62

87 | 30.6 | .0029 | .66

88 | 31.1 | .0031 | .70

-------+-------+-------+-----

[19] These temperature corrections are for a Brix instrument

standardized for 20°C. There are Brix hydrometers on the market

standardized for 17.5°C. Temperature corrections for a Brix hydrometer

standardized at this temperature may be obtained by correcting to

20° by means of the above table (for instrument graduated at 20°C.)

and adding to this corrected reading 0.12. For instance suppose the

reading for a 17.5° instrument is 7.00 at 25°C. The correction from

the above table will be .28 or a total of 7.28. Adding .12 to this

gives a corrected reading of 7.40. If the reading is 7.00 at 15°C.

the correction from the above table amounts to .22 (to be subtracted)

giving 6.78. Adding 0.12 to this gives the corrected reading of 6.90.

TABLE 9.—_Equivalent Volumes of Pulp of Different Degrees of

Concentration_

========================================================================

| | Factor by which to multiply volume of

Tomato pulp | Filtrate | pulp of given specific gravity to

| from pulp | ascertain volume of pulp with

| | equivalent solid content and with

| | specific gravity of

--------+-------+--------+-------+-------+-------+-------+-------+-------

Specific| Per |Specific|Degrees| | | | |

gravity | cent |gravity | Brix | | | | |

at |solids | at | at | 1.030 | 1.035 | 1.040 | 1.045 | 1.050

68° F. | | 68° F.| 68° F.| | | | |

--------+-------+--------+-------+-------+-------+-------+-------+-------

1.0125 | 2.79 | 1.0108 | 2.78 | .384 | .326 | .283 | .249 | .223

1.0130 | 2.92 | 1.0113 | 2.89 | .402 | .342 | .296 | .261 | .234

1.0135 | 3.05 | 1.0118 | 3.02 | .420 | .357 | .310 | .273 | .244

1.0140 | 3.17 | 1.0123 | 3.14 | .437 | .372 | .323 | .285 | .255

1.0145 | 3.30 | 1.0128 | 3.27 | .455 | .388 | .336 | .297 | .265

| | | | | | | |

1.0150 | 3.42 | 1.0133 | 3.40 | .472 | .401 | .348 | .306 | .274

1.0155 | 3.54 | 1.0138 | 3.51 | .489 | .416 | .361 | .318 | .284

1.0160 | 3.67 | 1.0143 | 3.65 | .507 | .431 | .374 | .329 | .294

1.0165 | 3.79 | 1.0148 | 3.77 | .524 | .445 | .387 | .341 | .304

1.0170 | 3.92 | 1.0153 | 3.90 | .542 | .460 | .400 | .352 | .315

| | | | | | | |

1.0175 | 4.05 | 1.0158 | 4.03 | .560 | .476 | .413 | .364 | .325

1.0180 | 4.18 | 1.0163 | 4.15 | .579 | .491 | .426 | .375 | .335

1.0185 | 4.30 | 1.0168 | 4.28 | .596 | .506 | .440 | .387 | .346

1.0190 | 4.43 | 1.0173 | 4.40 | .614 | .521 | .452 | .399 | .356

1.0195 | 4.56 | 1.0178 | 4.53 | .632 | .537 | .466 | .410 | .367

| | | | | | | |

1.0200 | 4.68 | 1.0182 | 4.63 | .649 | .551 | .478 | .421 | .377

1.0205 | 4.81 | 1.0188 | 4.77 | .667 | .566 | .491 | .433 | .387

1.0210 | 4.93 | 1.0192 | 4.87 | .684 | .581 | .504 | .444 | .398

1.0215 | 5.05 | 1.0196 | 4.97 | .701 | .596 | .517 | .456 | .407

1.0220 | 5.17 | 1.0201 | 5.10 | .718 | .610 | .529 | .467 | .417

| | | | | | | |

1.0225 | 5.30 | 1.0206 | 5.22 | .737 | .625 | .543 | .479 | .428

1.0230 | 5.43 | 1.0211 | 5.35 | .755 | .641 | .556 | .490 | .438

1.0235 | 5.55 | 1.0216 | 5.47 | .772 | .656 | .569 | .502 | .448

1.0240 | 5.67 | 1.0220 | 5.57 | .789 | .671 | .582 | .513 | .459

1.0245 | 5.80 | 1.0226 | 5.72 | .808 | .686 | .595 | .525 | .469

| | | | | | | |

1.0250 | 5.92 | 1.0230 | 5.82 | .825 | .701 | .608 | .536 | .479

1.0255 | 6.04 | 1.0235 | 5.94 | .842 | .715 | .620 | .547 | .489

1.0260 | 6.16 | 1.0240 | 6.07 | .859 | .729 | .633 | .558 | .499

1.0265 | 6.28 | 1.0244 | 6.17 | .876 | .744 | .646 | .569 | .509

1.0270 | 6.40 | 1.0249 | 6.29 | .894 | .759 | .658 | .580 | .519

| | | | | | | |

1.0275 | 6.53 | 1.0254 | 6.43 | .912 | .775 | .672 | .592 | .529

1.0280 | 6.65 | 1.0258 | 6.53 | .930 | .789 | .685 | .604 | .539

1.0285 | 6.77 | 1.0263 | 6.65 | .947 | .804 | .697 | .615 | .549

1.0290 | 6.90 | 1.0268 | 6.78 | .965 | .819 | .711 | .626 | .560

1.0295 | 7.02 | 1.0273 | 6.90 | .983 | .834 | .724 | .638 | .570

| | | | | | | |

1.0300 | 7.14 | 1.0278 | 7.03 | 1.000 | .849 | .737 | .649 | .580

1.0305 | 7.26 | 1.0282 | 7.13 | 1.017 | .864 | .749 | .660 | .590

1.0310 | 7.38 | 1.0287 | 7.23 | 1.035 | .878 | .762 | .672 | .600

1.0315 | 7.50 | 1.0292 | 7.35 | 1.052 | .893 | .775 | .683 | .610

1.0320 | 7.63 | 1.0296 | 7.45 | 1.071 | .908 | .788 | .695 | .621

| | | | | | | |

1.0325 | 7.75 | 1.0301 | 7.58 | 1.088 | .924 | .802 | .706 | .631

1.0330 | 7.88 | 1.0306 | 7.70 | 1.107 | .939 | .815 | .718 | .642

1.0335 | 8.00 | 1.0310 | 7.80 | 1.124 | .954 | .828 | .730 | .652

1.0340 | 8.12 | 1.0315 | 7.93 | 1.142 | .970 | .842 | .742 | .663

1.0345 | 8.25 | 1.0320 | 8.05 | 1.160 | .985 | .855 | .753 | .673

| | | | | | | |

1.0350 | 8.37 | 1.0325 | 8.16 | 1.178 | 1.000 | .868 | .765 | .684

1.0355 | 8.50 | 1.0330 | 8.27 | 1.197 | 1.016 | .882 | .777 | .695

1.0360 | 8.62 | 1.0334 | 8.37 | 1.214 | 1.031 | .895 | .788 | .705

1.0365 | 8.74 | 1.0339 | 8.50 | 1.232 | 1.046 | .907 | .800 | .715

1.0370 | 8.86 | 1.0344 | 8.63 | 1.249 | 1.061 | .920 | .811 | .725

| | | | | | | |

1.0375 | 8.98 | 1.0349 | 8.75 | 1.267 | 1.076 | .933 | .823 | .735

1.0380 | 9.10 | 1.0353 | 8.85 | 1.284 | 1.091 | .947 | .834 | .746

1.0385 | 9.23 | 1.0358 | 8.97 | 1.303 | 1.106 | .960 | .846 | .756

1.0390 | 9.35 | 1.0363 | 9.07 | 1.321 | 1.122 | .974 | .858 | .767

1.0395 | 9.48 | 1.0368 | 9.20 | 1.340 | 1.138 | .987 | .870 | .778

| | | | | | | |

1.0400 | 9.60 | 1.0372 | 9.30 | 1.358 | 1.153 | 1.000 | .881 | .788

1.0405 | 9.73 | 1.0378 | 9.45 | 1.377 | 1.168 | 1.014 | .893 | .799

1.0410 | 9.85 | 1.0383 | 9.57 | 1.394 | 1.184 | 1.027 | .905 | .809

1.0415 | 9.97 | 1.0387 | 9.67 | 1.412 | 1.199 | 1.041 | .917 | .820

1.0420 | 10.10 | 1.0393 | 9.80 | 1.431 | 1.215 | 1.054 | .929 | .830

| | | | | | | |

1.0425 | 10.22 | 1.0397 | 9.90 | 1.449 | 1.230 | 1.067 | .941 | .841

1.0430 | 10.35 | 1.0402 | 10.03 | 1.468 | 1.246 | 1.081 | .953 | .851

1.0435 | 10.47 | 1.0406 | 10.13 | 1.486 | 1.261 | 1.094 | .964 | .862

1.0440 | 10.60 | 1.0411 | 10.25 | 1.505 | 1.277 | 1.108 | .976 | .873

1.0445 | 10.72 | 1.0416 | 10.36 | 1.523 | 1.293 | 1.122 | .988 | .884

| | | | | | | |

1.0450 | 10.84 | 1.0420 | 10.45 | 1.540 | 1.308 | 1.135 | 1.000 | .894

1.0455 | 10.96 | 1.0425 | 10.57 | 1.558 | 1.322 | 1.148 | 1.012 | .904

1.0460 | 11.08 | 1.0429 | 10.67 | 1.576 | 1.338 | 1.161 | 1.023 | .915

1.0465 | 11.20 | 1.0435 | 10.83 | 1.594 | 1.353 | 1.174 | 1.035 | .925

1.0470 | 11.33 | 1.0440 | 10.93 | 1.613 | 1.369 | 1.188 | 1.047 | .936

| | | | | | | |

1.0475 | 11.45 | 1.0445 | 11.05 | 1.631 | 1.384 | 1.201 | 1.059 | .946

1.0480 | 11.57 | 1.0449 | 11.15 | 1.649 | 1.400 | 1.215 | 1.071 | .957

1.0485 | 11.70 | 1.0454 | 11.27 | 1.668 | 1.416 | 1.229 | 1.083 | .968

1.0490 | 11.82 | 1.0459 | 11.40 | 1.686 | 1.432 | 1.243 | 1.095 | .979

1.0495 | 11.95 | 1.0465 | 11.53 | 1.705 | 1.449 | 1.256 | 1.107 | .990

| | | | | | | |

1.0500 | 12.07 | 1.0468 | 11.60 | 1.724 | 1.464 | 1.270 | 1.119 | 1.00

1.0505 | 12.20 | 1.0474 | 11.75 | 1.743 | 1.479 | 1.284 | 1.131 | 1.01

1.0510 | 12.32 | 1.0478 | 11.84 | 1.761 | 1.495 | 1.298 | 1.144 | 1.02

1.0515 | 12.45 | 1.0482 | 11.93 | 1.780 | 1.511 | 1.311 | 1.156 | 1.03

1.0520 | 12.57 | 1.0488 | 12.07 | 1.797 | 1.526 | 1.325 | 1.167 | 1.04

| | | | | | | |

1.0525 | 12.69 | 1.0492 | 12.17 | 1.816 | 1.542 | 1.338 | 1.179 | 1.05

1.0530 | 12.81 | 1.0497 | 12.30 | 1.834 | 1.557 | 1.351 | 1.191 | 1.06

1.0535 | 12.93 | 1.0502 | 12.40 | 1.852 | 1.572 | 1.364 | 1.203 | 1.07

1.0540 | 13.05 | 1.0506 | 12.50 | 1.870 | 1.588 | 1.378 | 1.215 | 1.08

1.0545 | 13.18 | 1.0512 | 12.65 | 1.890 | 1.604 | 1.392 | 1.227 | 1.09

| | | | | | | |

1.0550 | 13.30 | 1.0516 | 12.74 | 1.908 | 1.620 | 1.405 | 1.239 | 1.10

1.0555 | 13.42 | 1.0520 | 12.83 | 1.926 | 1.635 | 1.419 | 1.250 | 1.11

1.0560 | 13.55 | 1.0525 | 12.95 | 1.945 | 1.651 | 1.433 | 1.263 | 1.12

1.0565 | 13.67 | 1.0529 | 13.05 | 1.964 | 1.667 | 1.447 | 1.275 | 1.14

1.0570 | 13.80 | 1.0534 | 13.16 | 1.983 | 1.684 | 1.461 | 1.288 | 1.15

--------+-------+--------+-------+-------+-------+-------+-------+-----

Tomato products: pulp, ketchup, and chili sauce. · 第 48 / 60 题