BORIC ACID.

Evaporate to dryness an aliquot portion of the alkaline filtrate (p.

61), treat the residue with 1 or 2 cc. of water, and slightly acidify

the solution with hydrochloric acid. Add about 25 cc. of absolute

alcohol, boil, filter, and repeat the extraction of the residue. Make

the filtrate slightly alkaline with sodium hydroxide, and evaporate it

to dryness. Add a little water, slightly acidify with hydrochloric acid,

and place a strip of turmeric paper in the liquid. Evaporate to dryness

on the steam bath, and continue the heating until the turmeric paper is

dry. If boric acid is present the turmeric paper becomes cherry red. It

is not usually necessary to determine quantitatively boric acid; the

quantitative method devised by Gooch[33] is recommended.

Standard methods for the examination of water and sewage · 第 139 / 249 题