DETERMINATION WITH GOOCH CRUCIBLE.

_Reagent._—Prepare a dilute cream of asbestos fibre which has been

finely shredded, thoroughly ignited, treated with strong hydrochloric

acid for at least 12 hours, and washed with distilled water till free

from acid.

_Procedure._—1. Prepare a mat of the asbestos fibre 1/16 inch thick in a

Gooch crucible. Dry it in an oven at 103 or 180° C., cool and weigh.

Filter 1,000 cc. of samples having a turbidity of 50 parts per million

or less. If the turbidity is higher use sufficient water to obtain 50 to

100 mg. of suspended matter. Dry for one hour at 103 or 180° C., cool

and weigh. Report the temperature at which the residue was dried. If

1,000 cc. is filtered the increase in weight expressed in milligrams is

equal to parts per million of suspended matter.

Standard methods for the examination of water and sewage · 第 53 / 249 题