FILM NEGATIVES.[1]

[Footnote 1: A communication to the Birmingham Photographic

Society.]

Having had a certain measure of success with Eastman stripping films,

I have been requested by your council to give a paper this evening

dealing with the subject, and particularly with the method of working

which my experience has found most successful. In according to their

request, I feel I have imposed upon myself a somewhat difficult task.

There is, undoubtedly, a strong prejudice in the minds of most

photographers, both amateur and professional, against a negative in

which paper is used as a permanent support, on account of the

inseparable "grain" and lack of brilliancy in the resulting prints;

and the idea of the paper being used only as a temporary support does

not seem to convey to their mind a correct impression of the true

position of the matter.

It may be as well before entering into the technical details of the

manipulation to consider briefly the advantages to be derived--which

will be better appreciated after an actual trial.

My experience (which is at present limited) is that they are far

superior to glass for all purposes except portraiture of the human

form or instantaneous pictures where extreme rapidity is necessary,

but for all ordinary cases of rapid exposure they are sufficiently

quick. The first advantage, which I soon discovered, is their entire

freedom from halation. This, with glass plates, is inseparable, and

even when much labor has been bestowed on backing them, the halation

is painfully apparent.

These films never frill, being made of emulsion which has been made

insoluble. Compare the respective weights of the two substances--one

plate weighing more than a dozen films of the same size.

Again, on comparing a stripping film negative with one on glass of the

same exposure and subject, it will be found there is a greater

sharpness or clearness in the detail, owing, I am of opinion, to the

paper absorbing the light immediately it has penetrated the emulsion,

the result being a brilliant negative. Landscapes on stripped films

can be retouched or printed from on either side, and the advantage in

this respect for carbon or mechanical printing is enormous. Now,

imagine the tourist working with glass, and compare him to another

working with films. The one works in harness, tugging, probably, a

half hundredweight of glass with him from place to place, paying extra

carriage, extra tips, and in a continual state of anxiety as to

possible breakage, difficulty of packing, and having to be continually

on the lookout for a dark place to change the plates, and, perhaps, on

his return finds numbers of his plates damaged owing to friction on

the surface; while the disciple of _films_, lightly burdened with only

camera and slide, and his (say two hundred) films in his pockets, for

they lie so compact together. Then the advantages to the tourists

abroad, their name is "legion," not the least being the ease of

guarding your exposed pictures from the custom house officials, who

almost always seek to make matters disagreeable in this respect, and

lastly, though not least, the ease with which the negatives can be

stowed away in envelopes or albums, etc., when reference to them is

easy in the extreme.

Now, having come (rightly, I think, you will admit) to the conclusion

that films have these advantages, you naturally ask, What are their

disadvantages? Remembering, then, that I am only advocating stripping

films, I consider they have but two disadvantages: First, they entail

some additional outlay in the way of apparatus, etc. Second, they are

a little more trouble to finish than the glass negatives, which sink

into insignificance when the manifold advantages are considered.

In order to deal effectively with the second objection I mentioned,

viz., the extra trouble and perseverance, I propose, with your

permission, to carry a negative through the different stages from

exposure to completion, and in so doing I shall endeavor to make the

process clear to you, and hope to enlist your attention.

The developer I use is slightly different to that of the Eastman

company, and is as follows:

A.

Sulphite of soda. 4 ounces.

To be dissolved in 8 ounces of hot distilled water, then rendered

slightly acid with citric acid, then add--

Pyrogallic acid. 1 ounce.

Water to make up to 10 ounces.

B.

Pure carbonate of soda. 1 ounce.

Water to make up in all to 10 ounces.

C.

Pure carbonate of potash. 1 ounce.

Water to make up to 10 ounces.

D.

Bromide of potassium. 1 ounce.

Water to make up to 10 ounces.

I have here two half-plate films exposed at 8:30 A.M. to-day, one with

five and one with six seconds' exposure, subject chiefly middle

distance. I take 90 minims A, 10 minims D, and 90 minims B, and make

up to 2 ounces water. I do not soak the films in water. There is no

need for it. In fact, it is prejudicial to do so. I place the films

face uppermost in the dish, and pour on the developer on the center of

the films. You will observe they lie perfectly flat, and are free from

air bubbles. Rock the dish continually during development, and when

the high lights are out add from 10 to 90 minims C, and finish

development and fix. The negatives being complete, I ask you to

observe that both are of equal quality, proving the latitude of

exposure permissible.

I now coat a piece of glass half an inch larger all round than the

negative with India rubber solution (see Eastman formula), and

squeegee the negative face downward upon the rubber, interposing a

sheet of blotting paper and oilskin between the negative and squeegee

to prevent injury to the exposed rubber surface, and then place the

negative under pressure with blotting paper interposed until

moderately dry only.

I then pour hot water upon it, and, gently rocking the dish, you see

the paper floats from the film without the necessity for pulling it

with a pin, leaving the film negative on the glass. Now, the

instructions say remove the remaining soluble gelatine with camel's

hair brush, but, unless it requires intensifying, which no properly

developed negative should require, you need not do so, but simply pour

on the gelatine solution (see Eastman formula), well covering the

edges of the film, and put on a level shelf to dry.

I will now take up a negative in this state on the glass, but dry, and

carefully cut round the edges of the film, and you see I can readily

pull off the film with its gelatine support. Having now passed through

the whole of the process, it behooves us to consider for a few minutes

the causes of failure in the hands of beginners and their remedies: 1.

The rubber will not flow over glass? Solution too thick, glass greasy.

2. Rubber peels off on drying? Dirty glass. 3. Negative not dense

enough? Use more bromide and longer development. 4. Gelatine cracks on

being pulled off? Add more glycerine. 5. Gelatine not thick enough?

Gelatine varnish too thin, not strong enough. 6. Does not dry

sufficiently hard? Too much glycerine.--_E.H. Jaques, Reported in Br.

Jour. of Photography._

* * * * *

HOW DIFFERENT TONES IN GELATINO-CHLORIDE PRINTS MAY BE VARIED BY

DEVELOPERS.

The following formulæ are for use with gelatino-chloride paper or

plates. The quantities are in each case calculated for one ounce,

three parts of each of the following solutions being employed and

added to one part of solution of protosulphate of iron. Strength, 140

grains to the ounce.

_Slaty Blue._

1.--One part of the above solution

to three parts of a solution of citrate of ammonia.

_Greenish Brown._

2.--Citric acid. 180 grains

Carbonate of ammonia. 50 "

3.--Citrate of ammonia. 250 grains.

Chloride of sodium. 2 "

4.--Citrate of ammonia. 250 grains.

Chloride of sodium. 4 "

_Sepia Brown._

5.--Citrate of ammonia. 250 grains.

Chloride of sodium. 8 "

_Clear Red Brown._

6.--Citric acid. 120 grains.

Carbonate of magnesia. 76 "

_Warm Gray Brown._

7.--Citric acid. 120 grains.

Carbonate of soda. 205 "

_Deep Red Brown._

8.--Citric acid. 120 grains.

Carbonate of potash. 117 "

_Green Blue._

9.--Citric acid. 90 grains.

Carbonate of soda. 154 "

Citrate of potash. 24 "

Oxalate of potash. 6 "

_Sepia Red._

10.--Citric acid. 80 grains.

Carbonate of soda. 135 "

Citrate of potash. 12 "

Oxalate of potash. 3 "

11.--Citric acid. 108 grains.

Carbonate of magnesia. 68 "

Carbonate of potash. 12 "

Oxalate of potash. 3 "

_Sepia Yellow._

12.--Citric acid. 40 grains.

Carbonate of magnesia. 25 "

Citrate of ammonia. 166 "

13.--Citric acid. 120 grains.

Carbonate of magnesia. 72 "

Carbonate of ammonia. 72 "

Chloride of sodium. 8 "

_Blue Black._

14.--Citric acid. 120 grains.

Carbonate of ammonia. 70 "

Carbonate of magnesia. 15 "

15.--Citric acid. 120 grains.

Carbonate of magnesia. 38 "

Carbonate of ammonia. 44 "

16.--Citric acid. 90 grains.

Carbonate of magnesia. 57 "

Citrate of potash. 54 "

Oxlate of potash. 18 "

17.--Citric acid. 72 grains.

Carbonate of magnesia. 45 "

Citrate of potash. 54 "

Oxalate of potash. 18 "

18.--Citric acid. 60 grains.

Carbonate of magnesia. 38 "

Citrate of potash. 68 "

Oxalate of potash. 22 "

_A more Intense Blue Black._

19.--Citric acid. 30 grains.

Carbonate of magnesia. 18 "

Citrate of potash. 100 "

Oxalate of potash. 33 "

_A Clearer Blue._

20.--Citrate of potash. 136 grains.

Oxalate of potash. 44 "

In the photographic exhibition at Florence, the firm of Corvan[1]

places on view a frame containing twenty proofs produced by the

foregoing twenty formulæ, in such a way that the observer can compare

the value of each tone and select that which pleases him best.--_Le

Moniteur de la Photographie, translated by British Jour. of Photo._

[Footnote 1: Does this mean Mr. A. Cowan?--_Translator._]

* * * * *

Scientific American Supplement, No. 623, December 10, 1887 · 第 14 / 34 题