MANUFACTURE OF PHOTOGRAPHIC SENSITIVE PLATES.

Quite recently Messrs. Marion & Company, London, began on their own

account to manufacture sensitive photographic plates by machinery, and

the operations are exceedingly delicate, for a single minute air

bubble or speck of dust on a plate may mar the perfection of a

picture. Their works for the purpose at Southgate were erected in the

summer of 1886, and were designed throughout by Mr. Alexander Cowan.

[Illustration: Fig. 1.]

Buildings of this kind have to be specially constructed, because some

of the operations have to be carried on in the absence of daylight,

and in that kind of non-actinic illumination which does not act upon

the particular description of sensitive photographic compound

manipulated. Glass and other materials have therefore to pass from

light to dark rooms through double doors or double sliding cupboards

made for the purpose, and the workshops have to be so placed in

relation to each other that the amount of lifting and the distance of

carriage of material shall be reduced to a minimum. Moreover, the

final drying of sensitive photographic plates takes place in absolute

darkness. Fig. 1 is a ground plan of the chief portion of the works.

In this cut, A is the manager's private office, B the counting house,

C the manager's laboratory, and D his dark room for private

experiment, which can thus be conducted without interfering with the

regular work of the establishment. E is the carpenter's shop and

packing room, F the albumen preparation room, G the engine room, with

its two doors; the position of the engine is marked at H. The main

building is entered through the door, K; the passage, L, is used for

the storage of glass, and has openings in the wall on one side to

permit the passage of glass into the cleaning room, M; this room is

illuminated by daylight. The plates, after being cleaned, pass into

the coating rooms, N and O, into which daylight is never admitted; the

coating machine is in the room, N, and three hand coating tables in

the room, O; both these rooms are illuminated by non-actinic light.

[Illustration: Fig. 2.]

[Illustration: Fig. 3.]

The walls of N and O are of brick, to keep these interior rooms as

cool as possible in hot weather, for the making of photographic plates

is more difficult in summer time, because the high temperature tends

to prevent the rapid setting of the gelatine emulsion upon them. At

the end of these rooms and communicating with both is the lift, P, by

which the coated plates are carried to the drying rooms above, which

there cover the entire area of the main building; they consist of two

rooms measuring 60 ft. by 30 ft., and are each 30 ft. high at the

highest part in the center of the building; these rooms are

necessarily kept in absolute darkness, except while the plates are

being stored therein or removed therefrom, and on such occasions

non-actinic light is used. After the plates are dry, they come down

the lift, Q, into the cutting and packing room, R, which is

illuminated by non-actinic light. In the drying rooms the batches of

plates are placed one after the other on tram lines at one end of the

room, and are gradually pushed to the other end of the building, so

that the first batches coated are the first to be ready to be taken

off when dry, and to be sent down the lift, Q. The plates in R, when

sufficiently packed to be safe from the action of daylight, are passed

through specially constructed openings into the outside packing room,

S, where they are labeled. The chemicals are kept in the room, U,

where they are weighed and measured ready for the making of the

photographic emulsion in the room, U. The next room, V, is for washing

small experimental batches of emulsion, and W is the large washing

room. The emulsion is then taken into the passage, X, communicating

with the two coating rooms. A centrifugal machine in the room, Y, is

used for extracting silver residues from waste materials, also for

freeing the emulsion from all soluble salts. Washing and cleaning in

general go on in the room, Z.

[Illustration: Fig. 4.]

The glass for machine coating is cut to standard sizes at the

starting, instead of being coated in large sheets and cut afterward--a

practice somewhat common in this industry. The disadvantage of the

ordinary plan is that minute fragments of glass are liable to settle

upon the sensitive film and to cause spots and scratches during the

packing operations; any defect of this kind renders a plate worthless

to the photographer. When any breakages take place in the cutting, it

is best that they should occur at the outset, and not after the plate

has been coated with emulsion. The cutting when necessary is effected

by the aid of a "cutting board," Fig. 2, invented by Mr. Cowan, and

now largely in use in the photographic world. This appliance is used

to divide into two equal parts, with absolute exactness, any plate

within its capacity, and it is especially useful in dimly lighted

rooms. It consists of four rods pivoted together at the corners and

swinging on two centers, so that in the first position it is truly

square, and in other positions of rhomboid form, the two outer bars

approaching each other like those of a parallel ruler. The hinge flap

comes down on the exact center of the plate, minus the thickness of

the block holding the diamond. By this appliance plates can be cut in

either direction. Fig. 3 represents a similar arrangement for cutting

a number of very small plates out of one large one; in this the hinge

flap is made in the form of a gridiron, and the bars are spaced at

accurate distances, according to the size of the plate to be cut, so

that a plate 10 in. square, receiving four cuts in each direction,

will be divided into twenty-five small plates.

[Illustration: Fig. 5.]

Before being cleaned all sharp edges are roughly taken off those

plates intended for machine coating by girls, who rub the edges and

corners of the plates upon a stone; the plates are then cleaned by any

suitable method in use among photographers. The plates, now ready for

the coating room, have to be warmed to the temperature of the

emulsion, say from 80 deg. F. to 100 deg. F., before they pass to the

coating machine, the inventor of which, Mr. Cadett, having come to the

conclusion that, if the plates are not of the proper temperature, the

coating given will be uneven over various parts of the surface. The

plate-warming machine is represented in Fig. 4; it was designed by Mr.

A. Cowan, and made by his son, Mr. A. R. Cowan. It consists of a

trough 7 ft. long by 3 in. deep, forming a flat tank, through which

hot water passes by means of the circulating system shown in the

engraving. To facilitate the traveling of the glass plates without

friction the top of the tank is a sheet of plate glass bedded on a

sand bath. An assistant at one end places the glasses one after the

other on the warm glass slab, and by means of a movable slide pushes

them one at a time under the cover, which cover is represented raised

in the engraving to show the interior of the machine. After having put

one glass plate on the slide, another cannot be added until the man in

the dark room at the other end of the slide has taken off the farthest

warmed plate, because the slide has a reciprocating movement. This

heating apparatus is built at right angles to the coating machine in

the next room, in order to be conveniently placed in the present

building; but it is intended in future to use it as a part of the

coating machine itself, and to drive it at the same speed and with the

same gearing, so that the cold plates will be put on by hand at one

end, get warmed as they pass into the dark room, at the other end of

which they will be delivered by the machine in coated condition.

Underneath the heating table is a copper boiler, with its Bunsen's

burner of three concentric rings to get up the temperature quickly and

to give the power of keeping the water under the heating slab at a

definite temperature, as indicated by a thermometer. The cold water

tank of the system is represented against the wall in the cut.

[Illustration: Fig. 6.]

Fig. 5 represents the hot water circulating system outside the coating

rooms for keeping the gelatine emulsions in these dimly lighted

regions at a given temperature, without liberating the products of

combustion where the emulsion is manipulated. The temperature is

regulated automatically. It will be noticed where the pipes enter the

two coating rooms, and Fig. 6 shows the copper inside one of them

heated by the apparatus just described. The emulsion vessel in the

copper is surrounded by warm water, and the copper itself is jacketed

and connected with the hot water pipes, so forming part of the

circulating system.

[Illustration: Fig. 7.]

Fig. 7 is a general view of the coating machine recently invented by

Mr. Cadett, of the Greville Works, Ashtead, Surrey. The plates warmed

in the light room, as already described, are delivered near the end of

the coating table, where they are picked off a gridiron-like platform,

represented on the right hand side of the cut, and are placed by an

assistant one by one upon the parallel gauges shown at the beginning

of the machine proper; they are then carried on endless cords under

the coating trough described farther on. After they have been coated

they are carried onward upon a series of four broad endless bands of

absorbent cotton--Turkish toweling answers well--and this cotton is

kept constantly soaked with cold water, which flows over sheets of

accurately leveled plate glass below and in contact with the toweling;

the backs of the plates being thus kept in contact with fresh cold

water, the emulsion upon them is soon cooled down and is firmly set by

the time the plates have reached the end of the series of four wet

tables. They are then received upon one over which dry toweling

travels, which absorbs most of the moisture which may be clinging to

the backs of the plates; very little wet comes off the backs, so that

during a day's work it is not necessary to adopt special means to

redry this last endless band. What are technically known as "whole

plates," which are 8½ in. by 6½ in., are placed touching each other

end to end as they enter the machine, and they travel through it at

the rate of 720 per hour; smaller sizes are coated in proportion, the

smaller the plates the larger is the number coated in a given time.

The smaller plates pass through the machine in two parallel rows,

instead of in a single row, so that quarter plates, 4¼ in. by 3¼ in.,

are delivered at the end of the machine at the rate of 2,800 per hour,

keeping two attendants well employed in picking them up and placing

them in racks as quickly as they can do the work. The double row of

cords for carrying two lines of small plates through the machine is

represented in the engraving. Although the plates touch each other at

their edges on entering the machine, they are separated from each

other by short intervals after being coated; this is effected by

differential gearing. The water flowing over the tables for cooling

the plates is caught in receptacles below and carried away by pipes.

Between each of the tables is a little roller to enable small plates

to travel without tilting over the necessary gap between each pair of

bands.

[Illustration: Fig. 8.]

The feeding trough of Cadett's machine is represented in Fig. 8. The

plates, cleaned as already described, are carried upon the cords under

a brass roller, the weight of which causes sufficient friction to keep

the plates from tilting; they next pass under a soft camel's hair

brush to remove anything in the shape of dust or grit, and are then

coated. They afterward pass over a series of accurately leveled wheels

running in a tank of water kept exact by an automatic regulator at a

temperature of from 80 deg. Fah. to 100 deg. Fah., by means of a small

hot water circulating system. The emulsion trough is jacketed with hot

water at a constant temperature. This trough is silver plated inside,

because most metals in common use would spoil the emulsion by chemical

action. The trough is 16 in. long; it somewhat tapers toward the

bottom, and contains a series of silver pumps shown in the cut; the

whole of this series of pumps is connected with one long adjustable

crank when plates of the largest size have to be coated; when coating

plates of smaller sizes some of the pumps are detached. A chief object

of the machine is to deliver a carefully measured quantity of emulsion

upon each plate, and this is done by means of pumps, in order that the

quantity of emulsion delivered shall not be affected by changes in the

level of the emulsion in the trough; the quantity delivered is thus

independent of variations due to gravity or to the speed of the

machine. These pumps draw the emulsion from a sufficient depth in the

trough to avoid danger from the presence of air bubbles, and the

bottom of the trough is so shaped that should by chance any

sedimentary matter be present, it has a tendency to travel downward,

away from the bottoms of the pumps. There is a steady flow of emulsion

from the pumps to the delivery pipes, then it passes down a guide

plate of the exact width of the plate to be coated. Immediately in

front of the guide plate is a fixed silver cylinder, kept out of

contact with the plate by the thickness of a piece of fine and very

hard hempen cord, which can be renewed from time to time. These cords

keep the cylinder from scraping the emulsion off the plate, and they

help to distribute it in an even layer. There would be two lines upon

each plate where it is touched by the cords, were not the emulsion so

fluid as to flow over the cut-like lines made and close them up.

[Illustration: Fig. 9.]

The silver cylinder to a certain extent overcomes the effects of

irregularities in the glass plates, for the cylinder is jointed

somewhat in the cup and ball fashion, and is made in two or more

parts, which parts are held together by lengths of India rubber.

The arrangement is shown in section in Fig. 9, in which A is the hot

water jacket of the emulsion vessel; B, the crank driving the pumps;

C, a pump with piston in position; D, delivery tube of the pump; E,

the silver guide plate to conduct the emulsion down to the glass; F,

the spreading cylinder; G, the cords regulating the distance of the

cylinder from the glass plates; H, soft camel's hair brush; K,

friction roller; L L L, three plates passing under the emulsion tank;

M, knife edged wheels in the hot water tank, N; the "plucking roller,"

P, has a hot water tank of its own, and travels at slightly greater

speed than the other rollers; R is the beginning of the cooling bands;

T, the driving cords; and W, a level of the emulsion in the trough. Y

represents one of the bucket pistons of the pumps, detached. The

construction of the crank itself is such that, by adjustment of the

connecting rods, more or less emulsion may be put upon the plates. Mr.

Cowan, however, intends to adjust the pumps once for all, and to

regulate the amount of emulsion delivered upon the plates by means of

driving wheels of different diameters upon the cranks.

[Illustration: Fig. 10.]

Fig. 10 is a section of the hollow spreading cylinder, made of sheet

silver as thin as paper, so that its weight is light. For coating

large plates it is divided in the center, so as to adapt itself

somewhat to irregularities in the surface of each plate. In this case

it is supported by a third and central thread, as represented in the

cut. Otherwise the cylinder would touch the center of the plate. Its

two halves are held together by a slip of India rubber.--_The

Engineer_.

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Scientific American Supplement, No. 647, May 26, 1888 · 第 31 / 59 题