Illustration: FIG. 3. (‡ SMALL PORTABLE CONDENSER.)

These are vessels of different kinds used in distilling, that

is, when any volatile product has to be converted into vapour and

afterwards condensed, for the purpose of separating it from various

matters not otherwise separable. One of the oldest forms of still is

that even yet used in most chemical operations, called the “retort”

(fig. 1). It is blown out of glass in one piece, is easily made

of all sizes, not exceeding a few gallons; it is chiefly used for

distilling small quantities of fluids, and those which act on metals,

as the acids. For some purposes, chiefly those requiring a very

high temperature, earthenware retorts are used, and in other cases

retorts made of platinum; the retort is often “tubulated,” a name

given to those with an orifice in the upper part having a stopper

fitted to it, this opening is useful to introduce any substance

while the body of the retort is already partly filled with its

contents, or to add more of anything from time to time as it distils

over. An indispensable adjunct to the retort is a “receiver” for

condensing the liquid distilled; this is generally of a globular

form, with an opening to receive the spout of the retort, which is

also frequently “tubulated” that it may be attached by a bent tube

to a second or third receiver. The receiver is to be kept cool, and

this is generally done by a stream of cold water being poured on

it, or a cloth dipped in cold water being spread over it, &c. The

stills properly so called, such as are used in the manufacture of

large quantities of liquids, as, for example, in the distillation

of spirit, are generally made of copper tinned inside to prevent

the formation of verdigris, and consist of a body, a head, and a

condenser, the common form of which is seen at fig. 2. The condenser

consists of a long tube coiled up into a spiral and placed in a

large tub of water, having a supply tube to let in cold water at the

bottom, and one for the exit of the hot water at the top, for hot

water being lighter than cold, rises up to the top of the tub. A very

good form for a small portable condenser may be seen at fig. 3, in

which a constant current of cold water is made to pass through the

outer tube, and so keep the inner one cold.

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