AN APPARATUS FOR HEATING SUBSTANCES IN GLASS TUBES UNDER PRESSURE.[1]

[Footnote 1: Read at the meeting of the Chemical Section of the

Franklin Institute held March 17, 1891.]

By H. PEMBERTON, Jr.

Chemists who do not happen to have in their laboratories oil or air

baths for heating closed tubes can make an air bath at short notice

from materials furnished by all dealers in steam fittings.

_Order_:

(1) One four-inch wrought iron pipe, eighteen inches out to out, with

usual thread on each end. At about nine inches from either end this

pipe is drilled and tapped for a one-inch nipple, in such a manner

that a pipe introduced would pass, not on a line with the radius, but

about half way between the axis of the four-inch pipe and its walls;

in other words, it would be on a line with a chord of the circle.

(2) One one-inch wrought iron nipple, two inches long, one-inch thread

on one end.

(3) Two four-inch malleable iron caps, drilled and tapped for a

one-inch pipe.

(4) One one-inch wrought iron pipe, twenty-four inches out to out,

with a three-inch straight thread on each end.

(5) Two one-inch iron caps. A hole, one-eighth of an inch in diameter,

is drilled in the end of one of these caps.

The above order can be given _literatim_, and will be understood by

the dealer, who will furnish, at a trifling cost, the materials, cut

and tapped as ordered.

Fig. 1 shows how the whole is put together. The numbers on the figure

correspond also to the numbers of the paragraphs of the order as given

above.

[Illustration: FIG. 1.]

[Illustration: FIG. 2.]

Fig. 2 is an end section. A cork is inserted in 2 and through it a

thermometer, the bulb of which is on a level with the interior pipe.

The whole is supported on a few bricks at either end, and is kept

steady and in place by a couple of weights or half bricks. It is

heated by one or two Bunsen burners, according to the temperature

desired.--_Jour. Fr. Institute_.

* * * * *

Scientific American Supplement, No. 803, May 23, 1891 · 第 40 / 48 题